Table T7. Analytical conditions for ICP-AES analyses.
Element | Wavelength (nm) |
Integration time per calculation point (s) |
Photomultiplier voltage (V) |
Photomultiplier gain |
Increment between points (nm) |
Number of calculation points |
Limit of detection (ppm) |
---|---|---|---|---|---|---|---|
Al† | 396.152 | 0.5 | 720 | 1 | 0.002 | 7 | 0.109 |
Ba | 455.403 | 0.5 | 730 | 10 | 0.002 | 7 | 10 |
Ca† | 393.366 | 0.5 | 350 | 1 | 0.002 | 7 | 0.084 |
Co | 228.616 | 0.5 | 990 | 100 | 0.002 | 7 | 39 |
Cr | 267.716 | 0.5 | 860 | 100 | 0.002 | 7 | 22 |
Cu | 324.754 | 0.5 | 690 | 10 | 0.002 | 7 | 112 |
Fe† | 259.940 | 0.5 | 560 | 10 | 0.002 | 7 | 0.328 |
K† | 766.490 | 0.5 | 990 | 100 | 0.002 | 7 | 0.014 |
Mg† | 285.213 | 0.5 | 600 | 10 | 0.002 | 7 | 0.220 |
Mn† | 257.610 | 0.5 | 580 | 100 | 0.002 | 7 | 0.016 |
Na† | 589.592 | 0.5 | 610 | 10 | 0.002 | 7 | 0.086 |
Ni | 231.604 | 0.5 | 990 | 100 | 0.002 | 7 | 55 |
P† | 178.229 | 0.5 | 990 | 100 | 0.002 | 7 | 0.143 |
Si† | 251.611 | 0.5 | 570 | 10 | 0.002 | 7 | 0.522 |
Sr | 407.771 | 0.5 | 560 | 10 | 0.002 | 7 | 2 |
V | 292.402 | 0.5 | 960 | 100 | 0.002 | 7 | 3 |
Y | 371.029 | 0.5 | 620 | 100 | 0.002 | 7 | 2 |
Zr | 343.823 | 0.5 | 640 | 100 | 0.002 | 7 | 6 |
Ti† | 334.941 | 0.5 | 570 | 10 | 0.002 | 7 | 0.021 |
Sc | 361.384 | 0.5 | 660 | 100 | 0.002 | 7 | 1 |
Notes: ICP-AES = inductively coupled plasma–atomic emission spectrometry. † = Limit of detection reported as oxide weight percent. Detection limits of the instrument represent three times the instrumental blank (See “Analysis” in “ICP-AES analyses of major and trace elements”).
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