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Table T9. Interstitial water analyses and budget, Expedition 346.

Analytes Method Model of instrument IW
volume
(mL)
Priority
Salinity Digital refractometer Index Instruments Ltd. 0.1 H
pH Gran titration Brinkman pH electrode Metrohm 794 basic Titrino autotitrator 3 H
Alkalinity        
Cl Titration against silver nitrate Metrohm 785 DMP Titrino autotitrator 0.1 H
SO42– Ion chromatography Metrohm 850 professional ion chromatograph 0.1 H
Br        
Cl        
Ca ICP-AES/Ion chromatography Teledyne Prodigy high-dispersion ICP-AES/Metrohm 850 professional ion chromatograph 4 H
K        
Mg        
Na        
Ba ICP-AES Teledyne Prodigy high-dispersion ICP-AES        
B        
Fe        
Li        
Mn        
Si        
Sr        
NH4+ Spectrophotometry Agilent Cary 100 UV-VIS spectrophotometer 3 H
PO43–        
H4SiO4        
HS     1 H*
Yellowness     1 H*
Isotopes (Mg, K, Ca) Shore-based water requirements     5 M
δ34S     5 M
δ13C     5 M
Archive IW     5 L

ICP-AES = inductively coupled plasma–atomic emission spectroscopy. IW = interstitial water. UV-VIS = ultraviolet-visible. H = high priority, H* = high priority in shallow sediment of gas-rich sequences, M = medium priority, L = low priority.

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