Table T9. Interstitial water analyses and budget, Expedition 346.
Analytes | Method | Model of instrument | IW volume (mL) |
Priority |
---|---|---|---|---|
Salinity | Digital refractometer | Index Instruments Ltd. | 0.1 | H |
pH | Gran titration | Brinkman pH electrode Metrohm 794 basic Titrino autotitrator | 3 | H |
Alkalinity | ||||
Cl– | Titration against silver nitrate | Metrohm 785 DMP Titrino autotitrator | 0.1 | H |
SO42– | Ion chromatography | Metrohm 850 professional ion chromatograph | 0.1 | H |
Br– | ||||
Cl– | ||||
Ca | ICP-AES/Ion chromatography | Teledyne Prodigy high-dispersion ICP-AES/Metrohm 850 professional ion chromatograph | 4 | H |
K | ||||
Mg | ||||
Na | ||||
Ba | ICP-AES | Teledyne Prodigy high-dispersion ICP-AES | ||
B | ||||
Fe | ||||
Li | ||||
Mn | ||||
Si | ||||
Sr | ||||
NH4+ | Spectrophotometry | Agilent Cary 100 UV-VIS spectrophotometer | 3 | H |
PO43– | ||||
H4SiO4– | ||||
HS– | 1 | H* | ||
Yellowness | 1 | H* | ||
Isotopes (Mg, K, Ca) | Shore-based water requirements | 5 | M | |
δ34S | 5 | M | ||
δ13C | 5 | M | ||
Archive IW | 5 | L |
ICP-AES = inductively coupled plasma–atomic emission spectroscopy. IW = interstitial water. UV-VIS = ultraviolet-visible. H = high priority, H* = high priority in shallow sediment of gas-rich sequences, M = medium priority, L = low priority.
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