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Table T2. Analytical methods and precisions for interstitial water geochemistry measurements, Expedition 303.

Parameter Method Precision
(%)
Alkalinity Gran titration 1.5
pH Gran titration 3.1
Cl Titration with AgNO3 0.2
SO42– Ion chromatography 2.0
Li+ ICP-AES 2.2
K+ Ion chromatography 1.6
NH4+ Spectrophotometer 2.5
Mg2+ Ion chromatography 2.7
Ca2+ Ion chromatography 5.2
Sr2+ ICP-AES 1.3
Ba2+ ICP-AES 27.1
Mn2+ ICP-AES 27.0
Fe2+ ICP-AES 62.1
H3BO3 ICP-AES 2.1
H4SiO4 ICP-AES 3.9

Note: The reproducibility of analytical techniques is expressed as 1σ standard deviation of the mean of multiple determinations of a standard. The standard data used to calculate analytical precision in this table were generated during the period of analyses for the samples from Sites U1302–U1307. ICP-AES = inductively coupled plasma–atomic emission spectroscopy.

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